腺苷和虫草素的测定

编号：C15000912                                 货号：152200542

填料：ATEO-C18                                  流动相：乙腈/水=5/95

柱长：0.25m                                     柱压：12.5MPa 

内径：4.6mm                                     波长：260nm 

粒径：5μm                                      流量：1.0mL/min 

样品：蛹虫草子实体粉样品                        进样体积：10μL 

温度：35℃                                      适用PH：2-8

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保留时间     名称       峰面积       峰分离度     理论塔板数     峰拖尾因子

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4.889                  556381        4.68         61155           1.06      

7.575                  254524        3.75         48489           0.99      

8.947       腺苷       124970        1.24         46121           1.19      

18.352      虫草素     474951        1.03         55479           0.91      

25.152                 165383        1.24         54056           0.90      

38.722                 341793        0.00         63402           0.92      

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填料：ATEO-C18-AQ                               流动相：乙腈/水=5/95

柱长：0.25m                                     柱压：16.5MPa 

内径：4.6mm                                     波长：260nm 

粒径：5μm                                      流量：1.0mL/min 

样品：蛹虫草子实体粉样品                        进样体积：10μL 

温度： 35℃                                     适用PH：2-8

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保留时间         名称      峰面积       峰分离度    理论塔板数    峰拖尾因子

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6.672                      200876       3.38        35870          1.15      

7.648          腺苷        87080        17.16       45430          1.10      

14.778         虫草素      395789       9.31        49559          0.94      

20.438                     99522        0.00        60269          0.94      

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